Avance NEO 400 WB DNP Wissembourg
Sonde 3.2mm LT-MAS DNP
DR Mode, 1H, 13C-29Si
07/02/2018
Sample 6, MMM Beta Zeolite with template in 20 uL TEKPol TCE (20 mM) wetness impregnation
rotation 12.5 kHz BP = 2400 DP = 1500
T sample 99 K, flow = 1870 l/h, Tb = 100 K, Td = 110 K
1H13C CP
1H rf = 100 kHz, 2.5 us, 59 W
13C rf =35W, 4 us, 62.5 kHz
1H at 90 Khz, 48 W matched to 13C at 78 Khz, 55 W
D2 = 3.5s ns = 64
microwaves Off